CAS 102191-92-4|(TERT-BUTYLDIMETHYLSILYLOXY) ACETALDEHYDE
Fòmil molekilè: C8H18O2Si
Pwa molekilè: 174.31
Pite: 97 pousan Min.
Pake: 1 g / 5 g / 25 g / 100 g / 1 kg / 25 kg
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Spesifikasyon CAS 102191-92-4|(TERT-BUTYLDIMETHYLSILYLOXY) ACETALDEHYDE
ATIK | SPESIFIKASYON |
Pwen k ap fonn | 165-167 ºC |
Koulè | Blan nan limyè bèlj ak gri |
Tanperati depo. | 2-8 degre |
Fp | 140 degre F |
Endèks refraktif | n20/D 1.432(lit.) |
Fòm | Poud |
InChiKey | MEBFFOKESLAUSJ-UHFFFAOYSA-N |
Dansite | 0.915 g/mL nan 25 degre (lit.) |
Pwen bouyi | 165-167 degre (lit.) |
Espesifik gravite | 0.915 |
Sansiblite idrolitik | 8 |
Sentèz deCAS 102191-92-4|(TERT-BUTYLDIMETHYLSILYLOXY) ACETALDEHYDE
Kondisyon
Etap # 1: 2- (tèt-butildimetilsililoksi) etanòl Avèk dichloride oksalil Nan diklorometan; dimethyl sulfoxide nan -78 degre; pou 0.833333h; Swern oksidasyon; Atmosfè inaktif;
Etap #2: Avèk triethylamine Nan dichloromethane; dimethyl sulfoxide nan 20 degre; Atmosfè inaktif;
Referans
Cornil, Johan; Echeverria, Pierre-Georges; Reymond, Sébastien; Fansavath, Fannarath; Ratovelomanana-Vidal, Virginie; Guérinot, Amandine; Cossy, Janine
[Lèt òganik, 2016, vol. 18, # 18, p. 4534 - 4537]
Baj popilè: cas 102191-92-4|(tèt-butyldimethylsilyloxy) acetaldehyde, pri, sitasyon, rabè, nan stock, pou vann
